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NMR Solvent List

Solvent 1H Shift (ppm from TMS) 13C Shift (ppm from TMS) Water Resonance
( ppm)
Freezing Point
 
oC
Boiling Point
 
oC
Acetic Acid-d4 11.70(1), 2.05(5) 179.0, 20.7(7) - 17 118
Acetone-d6 2.05(5) 206.7, 29.8(7) 2.8 -94 57
Acetonitrile-d3 1.94(5) 118.7, 1.39(7) 2.1 -45 82
Benzene-d6 7.23(1) 128.0(3) 0.4 5 80
Chloroform-d 7.27(1) 77.0(3) 1.5 -64 62
Deuterium Oxide 4.86 none  DSS =-1.86ppm - 4 101
Dimethylformamide-d7 8.03(1), 2.92(5), 2.72(5) 163.0, 34.9(7), 29.8(7) 3.5 -61 153
DMSO-d6 2.50(5) 39.5(7) 3.3 18 189
Dioxane-d8 3.53(mult) 66.7(5) 2.4 12 101
Ethanol-d6 5.20(1), 3.56(3), 1.20(5) 57.0(5), 17.3(7) - -130 79
Methanol-d4 4.87(1), 3.31(5) 49.0(7) - -98 65
Methylene Chloride-d2 5.31(3) 54.0(5) 1.5 -95 40
Pyridine-d5 8.74, 7.58, 7.22 150.4(3), 135.9(3), 123.9(3) 5.0 -42 116
Tetrachloroethane-d2 5.99 73.8(3) 1.6 -44 147
THF-d8 3.58, 1.73 67.5(5), 25.4(5) 2.4 -109 66
Trichloroacetic acid-d 11.50 164.2(4), 116.6(4)   -15 72